Preparation of Ethyl Magnesium Bromide for Regiospecific Analysis of Triacylglycerols

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Preparation of ethyl magnesium bromide for regiospecific analysis of triacylglycerols.

This paper presents a procedure for preparation of a Grignard reagent, ethyl magnesium bromide, used for partial deacylation of triacylglycerols (TAG) in their regiospecific analysis. Magnesium turnings were reacted with ethereal solution of bromoethane in a screw-capped test tube to synthesize 2 mL of 1 M ethyl magnesium bromide. Continuously stirred with a vortex mixer, the reaction smoothly ...

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ژورنال

عنوان ژورنال: Journal of Oleo Science

سال: 2008

ISSN: 1345-8957,1347-3352

DOI: 10.5650/jos.57.459